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Posted By: Sree.... Member Level: Diamond Posted Date: 14 Jun 2008
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2006 Andhra Pradesh State Jawaharlal Nehru Technological University B.Tech ANALYTICAL INSTRUMENTATION Set No. 4 Question paper
Code No: RR411001 Set No. 4 IV B.Tech I Semester Supplementary Examinations, March 2006 ANALYTICAL INSTRUMENTATION (Electronics & Instrumentation Engineering) Time: 3 hours Max Marks: 80 Answer any FIVE Questions All Questions carry equal marks
1. With neat sketches explain the various methods for the measurement of electrolytic conductance. [16] 2. (a) Explain about the polarographic method of estimation of dissolved oxygen. (b) Give the application for polarographic oxygen analyzer. [10+6] 3. Compare and list out the merits and demerits of non-dispersive infrared analyzer over gas chromatography in carbon monoxide estimation. [16] 4. (a) With neat sketches, explain with detail Helium Ionization detector used in process gas chromatography system. (b) Compare & contrast Liquid chromatography with Process gas chromatogra- phy? [8+8] 5. Briefly explain absorption and interference filters Compare between grating and prism monochromators. [16] 6. (a) What is a filter? Mention the two types of filters generally used? (b) Explain briefly Absorption type of filter with a colorimetric setup. [6+10] 7. With neat block diagram, explain about the constructional details of NMR spec- trometer. [16] 8. Explain the constructional details and principle of operation of (a) surface barrier detector. (b) lithium drifted germanium detector. [8+8]
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