(5061104) Analytical Instrumentation
Teaching scheme: 3 lectures/week Credits: 3
Exam scheme: Paper- 100 marks
1. Introduction: Introduction to chemical analysis, Classical and Instrumental methods, Classification
of Instrumental techniques, important considerations in evaluating an instrumental method,
2. Absorption methods:
a. Spectrometric UV and VIS methods: Laws of photometry, Instrumentation.
b. IR spectrometry: correlation of IR spectra with molecular structure, Instrumentation.
c. Atomic absorption spectrometry: Principle, Instrumentation
3. Emission methods: Flame, AC/DC arc, spark, plasma excitation sources, instrumentation
4. Spectrofluroscence and phosphorescence spectrometer: Instrumentation, Raman spectrometer.
5. Mass spectrometer: Ionisation methods, mass analysers, mass detectors, FTMS.
6. Chromatography: Classification, Gas chromatography, Liquid chromatography, Instrumentation
7. X-ray and Nuclear methods: x-ray absorption, fluorescence and diffractometric techniques, electron
microscope and microprobe, ESCA and Auger techniques, nuclear radiation detectors.
8. NMR spectroscopy: Principle, chemical shift, spin-spin coupling, instrumentation, types of NMR.
9. Electroanalytical methods: potentiometry, voltammetry, coulometry techniques.
Text books:
1. Willard, Merritt, Dean and Settle, Instrumental Methods of Analysis, 7th edition, (CBS
publishers, New Delhi).
2. Galen W. Ewing, Instrumental Methods of Chemical Analysis, 5th edition, (McGraw-Hill Book
Company)
Reference http://www.unipune.ernet.in/stud_info/Syllabi/Syllabus_2008.html
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