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JNTU 2007-08 II Year II Sem B.Pharmacy - PHARMACEUTICAL ANALYSIS – I
Posted Date: 29 Dec 2007 Resource Type: Articles/Knowledge Sharing Category: Syllabus
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Posted By: India Member Level: Diamond
Rating:  Points: 1
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JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY
HYDERABAD
II Year B. Pharmacy II-Semester T P C
4+1* 0 4
(R7302) PHARMACEUTICAL ANALYSIS – I
UNIT –I
Computation of analytical results, significant figures, concept of error, precision, accuracy, standard deviation, rejection of doubtful values with special reference to volumetric analysis.
Calibration of analytical equipment used in volumetric analysis.
UNIT-II
(a) Theory of Neutralization Titration: Acidimetry, Alkalimetry, Acid-base concept, Common ion effect and Solubility product, pH, Buffers and indicators.
(b) General Principles and theory of oxidation-reduction methods, and precipitation methods. An account of the indicators used in these titrations.
Application of the above methods in the analysis of drugs, as under IP 1996 including the latest addendum.
UNIT -III
a) Complexometric titration: Theory, types and application in pharmaceutical analysis. Masking and demasking and their applications.
b) Non-aqueous Titration: Theory, types, solvents used and application in pharmaceutical analysis.
c) Karl-Fisher method of estimation of water and other methods of moisture determination.
Note: Principle, instrumentation and applications of instruments mentioned in UNIT IV to UNIT VI
UNIT - IV
Potentiometry, pH metry (including specific ion electrons), conductometry and polarography.
UNIT - V
Flourimetry, flame photometry, nephelometry & turbidometry.
UNIT – VI
Refractometry, polarimetry and spectropolarimetry.
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Responses
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| Author: India 29 Dec 2007 | Member Level: Diamond Points : 5 | TEXT BOOKS
1. Kasture & Wadodkar, Text Book of Pharmaceutical analysis Vol.I & II.
2. A. Day Under Wood, Text Book of Quantative Analysis
3. Connors, A Textbook of Pharmaceutical Analysis.
4. B.K. Sarma, Instrumental Chemical Analysis, Goel Publishers.
5. Chatwal & Anand, Instrumental Methods of Analysis.
REFERENCE
1. A.H. Beckett & J.B Stanlake Vol.I&II., Practical Pharmaceutical Chemistry, Athlone Press of the Univ of London
2. A.I Vogel, Quantitative Chemical Analysis, ELBS ed.
3. L M. Atherden, Bentley and Driver’s Textbook of Pharmaceutical Chemistry., Oxford University Press, Delhi.
4. Pharmacopoeia (IP, BP, USP).
5. Y.Anjaneyulu, K.Chandrasekhar, Valli Manickam, A Textbook of Analytical Chemistry
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